Materials analysis and pyrolysis

Make complex materials measurable.

Thermal sample preparation opens up direct access to polymers, lacquers, adhesives and unknown solids – without complicated extraction.

Thermal desorption

Our thermal desorption solutions compared

Thermal desorption: OPTIC-5, PAL3 TDAS 2020 and MARKES TD100-xr compared. Sample introduction, automation and manual handling; manual MARKES operation with UNITY-xr.
Comparison of sample introduction, automation and manual handling. Manual MARKES operation refers to UNITY-xr.

Pyrolysis

Our pyrolysis solutions compared

From rapid micro-pyrolysis to automated large-volume pyrolysis – the right technology for your analytical requirements.

Comparison of pyrolysis principle, method, sample amount, temperature, heating rate, automation, transfer and applications
CriterionGL Sciences OPTIC-5 PyroCHROMTECH Large Volume Pyrolysis
Pyrolysis principleDirect pyrolysis in the GC inletExternal furnace pyrolysis with a heated transfer line
MethodPy-GCMS – pyrolysis with GC-MSFurnace pyrolysis with GC-MS
Sample amountSmall samplesLarger samples; aluminium oxide crucibles with 600 or 900 µL
TemperatureUp to 1,000 °C in the Pyro versionUp to 1,000 °C
Heating rateUp to 100 °C/sUp to 30 °C/min
AutomationPAL RTC with LINEX liner exchangePAL RSI for up to 80 crucibles; PAL RTC for liner transfer
Pyrolysate transferDirect transfer into the GC systemHeated transfer line and sorbent collection; followed by thermal desorption in the OPTIC-5
Typical applicationsPolymer identification, materials characterisation and microplasticsThermal extraction/desorption with GC-MS or GC-MS/MS (TED); microplastics in environmental samples and heterogeneous samples

The appropriate sample mass depends on the material and method. Crucible volume does not specify a fixed sample mass. Temperatures and heating rates are instrument-specific maximum values.

Typical issues

From identification to quality control.

Polymer identificationAdditives and plasticizersCoatingsError and damage analysisThermal desorption

Material analysis

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